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U.N.C.L.E. official Robert Kingsley disappears, intending to conquer the world for good by using a docility gas. He's unaware that Thrush is using his wife to betray him.
A British U.N.C.L.E. agent is getting married. However, a Thrush commander, Koehler, kidnaps the man's fiancee and forces him to steal the plans for a supersubmarine.
With time running out, Napoleon and Illya face a firing squad when they fail to convince the "Seven Wonders" to turn against Kingsley and Thrush.